暂无反应条件数据

1: 84 percent / triethylamine / CH2Cl2 / 4 h / 0 °C 2: 2 N aq. HCl / acetic acid / 4 h / 120 °C View Scheme

1: 84 percent / triethylamine / CH2Cl2 / 4 h / 0 °C 2: 2 N aq. HCl / acetic acid / 4 h / 120 °C View Scheme

1: 75 percent / NaHCO3 / ethyl acetate; H2O / 0.5 h / 0 °C 2: 95 percent / K2CO3 / dimethylformamide / 1 h / Ambient temperature View Scheme

1: 75 percent / NaHCO3 / ethyl acetate; H2O / 0.5 h / 0 °C 2: 95 percent / K2CO3 / dimethylformamide / 1 h / Ambient temperature 3: 1) NaH / 1) DMF, 10 min, r.t., 2) DMF, 30 min, cooling 4: 100 percent / P2S5 / toluene / 2 h / Heating 5: 67 percent / 2 N NaOH / dioxane; methanol / 0.5 h View Scheme

1: NaOH-solution 2: water; ammonia / 100 °C View Scheme

ammonia; water