1.1: 3-chloro-benzenecarboperoxoic acid / ethylene glycol dimethyl ether / 2 h / 20 °C / |Cooling with ice 1.2: pH 9 2.1: 1,1,1,3,3,3-hexamethyl-disilazane; trimethylsilyl iodide / tetrahydrofuran / 5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Almirall, S.A.; Vidal Juan, Bernat; Alonso Diez, Juan Antonio; Buil Albero, María Antonia; Eastwood, Paul Robert; Esteve Trias, Cristina; Lozoya Toribio, María Estrella; Roberts, Richard Spurring; Vidal Gispert, Laura
Patent: EP2548876 A1, 2013 ;
EP 2548876 A1