2-甲基-6-庚烯-3-炔-2-醇合成路线 （共 12 条）
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; Copper(I)chloride in acetonitrile
参考文献
Loyola University of Chicago
Patent: US5231232 A1, 1993 ;
反应条件
copper(l) iodide; potassium carbonate; sodium sulfite; 1,8-diazabicyclo[5.4.0]undec-7-ene in dimethyl sulfoxide T=30°C; 4 h;
参考文献
Bieber, Lothar W.; da Silva, Margarete F.
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7088 - 7090
反应条件
1: 2-methyl-but-3-yn-2-ol With copper(l) iodide; potassium carbonate; triethylamine in N,N-dimethyl-formamide 2 h; 2: 3-chloroprop-1-ene in N,N-dimethyl-formamide T=50 - 55°C; 8 h; Further stages.;
参考文献
Veliev; Agaev; Shatirova; Chalabieva; Geidarova; Alieva
Russian Journal of Applied Chemistry, 2006 , vol. 79, # 11 p. 1829 - 1834
参考文献
Catellani,M. et al.
Journal of Organometallic Chemistry, 1978 , vol. 146, p. C19 - C22
参考文献
Bertrand
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1958 , vol. 247, p. 824,826
反应条件
(i) MeLi, THF, Et2O, (ii) /BRN= 605308/, (iii) aq. MeOH, TsOH; Multistep reaction;
参考文献
Karlsen; Froyen; Skattebol
Acta Chemica Scandinavica, 1976 , vol. 30, # 7 B p. 664 - 668
反应条件
1: HgSO4 / H2O / 10 °C 2: H2 / Raney-Ni / ethanol 3: H2 / Raney-Ni View Scheme
参考文献
Colonge,J.; Varagnat,A.
Bulletin de la Societe Chimique de France, 1964 , p. 2499 - 2504
反应条件
(i) HgSO4, (ii) (hydrogenation); Multistep reaction;
参考文献
Colonge,J.; Varagnat,A.
Bulletin de la Societe Chimique de France, 1964 , p. 2499 - 2504
参考文献
Colonge,J.; Varagnat,A.
Bulletin de la Societe Chimique de France, 1964 , p. 2499 - 2504
参考文献
Colonge; Falcotet
Bulletin de la Societe Chimique de France, 1957 , p. 1166
