Z-LEU-GLY-OH合成路线 (共 16 条)
反应条件
methanol; palladium; acetic acid Hydrogenation;
参考文献
Bergmann; Zervas; Fruton
Journal of Biological Chemistry, 1935 , vol. 111, p. 225,243
Journal of Biological Chemistry, 1936 , vol. 115, p. 593,596, 599
反应条件
1: 57 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
2: 100 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1,4-dioxane; sodium hydroxide
参考文献
Grassmann; Wuensch
Chemische Berichte, 1958 , vol. 91, p. 449,453
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Voss,H.
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, 1965 , vol. 20, p. 116 - 121
反应条件
1: 52 percent / Et3N / CH2Cl2 / 4 h / 0 °C
2: Jones' reagent / acetone / 3 h / 0 °C
3: 57 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
4: 100 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: Jones' reagent / acetone / 3 h / 0 °C
2: 57 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
3: 100 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: 52 percent / Et3N / CH2Cl2 / 4 h / 0 °C
2: Jones' reagent / acetone / 3 h / 0 °C
3: 57 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
4: 100 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: Et3N
2: aq. NaHCO3 / dimethylformamide
View Scheme
参考文献
Greben',A.E. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1968 , vol. 38, p. 664 - 665,639 - 640
反应条件
sodium hydroxide in 1,4-dioxane
参考文献
Bespalova,Zh.D. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1974 , vol. 44, # 1 p. 207 - 215,198 - 204
反应条件
sodium hydroxide
unter Kuehlung;
参考文献
Bergmann; Zervas; Fruton
Journal of Biological Chemistry, 1935 , vol. 111, p. 225,243
Journal of Biological Chemistry, 1936 , vol. 115, p. 593,596, 599