3,5-二硝基苯甲酸甲酯合成路线 （共 42 条）
反应条件
thionyl chloride T=0 - 20°C;
参考文献
COMENTIS, INC.; PURDUE RESEARCH FOUNDATION
Patent: WO2009/42694 A1, 2009 ;
Location in patent: Page/Page column 99 ;
WO 2009/042694 A1
反应条件
triethylamine in tetrahydrofuran Reflux;
参考文献
Wang, Chao; Yin, Shouchun; Chen, Senlin; Xu, Huaping; Wang, Zhiqiang; Zhang, Xi
Angewandte Chemie - International Edition, 2008 , vol. 47, # 47 p. 9049 - 9052
反应条件
1: (hydroxymethyl)dimethylphenylsilane With potassium tert-butylate; N,N,N',N'-tetramethyl-urea T=20 - 25°C; Brook rearrangement; 2: 3,5-dinitrobenzoic acid chloride With pyridine in tetrahydrofuran T=50°C; 1.5 h;
参考文献
Simov, Biljana Peric; Wuggenig, Frank; Mereiter, Kurt; Andres, Hendrik; France, Julien; Schnelli, Peter; Hammerschmidt, Friedrich
Journal of the American Chemical Society, 2005 , vol. 127, # 40 p. 13934 - 13940
反应条件
2,6-dimethylpyridine T=125°C; 96 h; Yields of byproduct given;
参考文献
Paquette,L.A.; Ohkata,K.; Jelich,K.
Journal of the American Chemical Society, 1983 , vol. 105, p. 2800
反应条件
potassium carbonate in acetonitrile 5 h; Heating;
参考文献
Yoshino, Tomonori; Togo, Hideo
Synlett, 2005 , # 3 art. no. U29304ST, p. 517 - 519
反应条件
in methanol; diethyl ether; toluene T=20°C; 1 h;
参考文献
Legouin, Beatrice; Gayral, Maud; Uriac, Philippe; Cupif, Jean-Francois; Levoin, Nicolas; Toupet, Loic; Van De Weghe, Pierre
European Journal of Organic Chemistry, 2010 , # 28 p. 5503 - 5508
反应条件
toluene-4-sulfonic acid in benzene
参考文献
Hosangadi, Bhaskar D.; Dave, Rajesh H.
Tetrahedron Letters, 1996 , vol. 37, # 35 p. 6375 - 6378
反应条件
2,6-dimethylpyridine T=125°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Paquette,L.A.; Ohkata,K.; Jelich,K.
Journal of the American Chemical Society, 1983 , vol. 105, p. 2800
反应条件
hydrogenchloride in acetone
参考文献
Monk, Keith A.; Siles, Rogelio; Pinney, Kevin G.; Garner, Charles M.
Tetrahedron Letters, 2003 , vol. 44, # 19 p. 3759 - 3761
反应条件
2,6-dimethylpyridine T=80°C; 48 h; Yield given. Yields of byproduct given;
参考文献
Paquette,L.A.; Ohkata,K.; Jelich,K.
Journal of the American Chemical Society, 1983 , vol. 105, p. 2800
