(3beta,7beta,17beta)-雄甾-5-烯-3,7,17-三醇合成路线 (共 8 条)
反应条件
Mortierella isabellina AM212 fungal strain 24 h; Enzymatic reaction;
参考文献
Milecka-Tronina, Natalia; Kolek, Teresa; Swizdor, Alina; Panek, Anna
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 2 p. 883 - 891
反应条件
sodium tetrahydroborate; cerium(III) chloride in methanol; dichloromethane T=0 - 5°C; pH=15; 0.5 h;
参考文献
Marwah, Padma; Marwah, Ashok; Lardy, Henry A.; Miyamoto, Hiroshi; Chang, Chawnshang
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 17 p. 5933 - 5947
反应条件
potassium hydroxide; sodium chloride in tetrahydrofuran; methanol
参考文献
Virginia Commonwealth University
Patent: US5206008 A1, 1993 ;
反应条件
Mucor silvaticus in acetone T=28°C; 96 h; regioselective reaction;
参考文献
Wang, Yanjie; Sun, Dongmei; Chen, Zhibao; Ruan, Hongsheng; Ge, Wenzhong
Biocatalysis and Biotransformation, 2013 , vol. 31, # 4 p. 168 - 174
反应条件
aluminum isopropoxide; isopropyl alcohol Abdestillieren des entstehenden Acetons;
参考文献
Schering A.G.
Patent: US2170124 , 1936 ;
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Schering-Kahlbaum A.G.
Patent: GB486854 , 1936 ;
Full Text Show Details
Butenandt; Hausmann; Paland
Chemische Berichte, 1938 , vol. 71, p. 1316,1321
反应条件
1: CrO3; aqueous acetic acid / 60 °C 2: aluminium isopropylate; isopropyl alcohol / Abdestillieren des entstehenden Acetons View Scheme
参考文献
Butenandt; Hausmann; Paland
Chemische Berichte, 1938 , vol. 71, p. 1316,1321
反应条件
Mortierella isabellina AM212 fungal strain 12 h; Enzymatic reaction;
参考文献
Kolek, Teresa; Milecka, Natalia; Swizdor, Alina; Panek, Anna; Bialonska, Agata
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5414 - 5422
反应条件
unter Abdestillieren des entstehenden Acetons;
参考文献
Schering A.G.
Patent: US2170124 , 1936 ;
Full Text Show Details
Butenandt; Hausmann; Paland
Chemische Berichte, 1938 , vol. 71, p. 1316,1321