in diethyl ether
byproducts: SO2, SO3; to finely ground dry Ag salt in anhyd. Et2O cooled to 0°C added dropwise with vigorous stirring equimolar amt. of thionyl chloride; suspn. stirred for 15 min; soln. was decanted from AgCl; AgCl dried; soln. washed (Et2O); all extracts combined; cooled to 0°C;
参考文献
Bondarenko; Gavrilova; Tikhanushkina; Zyk
Russian Chemical Bulletin, 2005 , vol. 54, # 9 p. 2145 - 2149
Noyes, W. A.
Journal of the American Chemical Society, 1930 , vol. 52, p. 4298
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Gmelin Handbook: N: MVol.3, 2.5.3, page 725 - 729