[1,3]二氧杂环戊并[4,5-g]异喹啉合成路线 （共 28 条）
反应条件
hydrogenchloride in 1,4-dioxane
22 h; Heating;
参考文献
Chantimakorn, Vilai; Nimgirawath, Surachai
Australian Journal of Chemistry, 1989 , vol. 42, # 1 p. 209 - 213
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in acetonitrile
T=0 - 20°C; 2.16667 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
1: 94 percent / PPh3, Et3N / PdCl2(PhCN)2 / 2.5 h / Heating
2: 95 percent / 10 percent aq. KOH / methanol / 0.58 h / 25 °C
3: NH2OH*HCl, pyridine / ethanol / 36 h / 25 °C
4: 1,2-dimethoxy-ethane / 120 h / Heating
View Scheme
参考文献
Grotjahn; Vollhardt
Synthesis, 1993 , # 6 p. 579 - 605
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane
T=20°C; 5 h; Title compound not separated from byproducts;
参考文献
Hung; Mooney; Prager; Ward
Australian Journal of Chemistry, 1981 , vol. 34, # 1 p. 151 - 162
反应条件
1: 94 percent / iodosylbenzene / tetrabutylammonium iodide / acetonitrile / 0.25 h / 0 °C
2: iodosylbenzene; [Bu4N]I / acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in acetonitrile
T=20°C; 1 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
benzophenone in benzene
24 h; Irradiation;
参考文献
Kessar, S V; Mankotia, Anil K Singh; Gujral, Gurjeet
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 5 p. 525 - 526
反应条件
1: 95 percent / 10 percent aq. KOH / methanol / 0.58 h / 25 °C
2: NH2OH*HCl, pyridine / ethanol / 36 h / 25 °C
3: 1,2-dimethoxy-ethane / 120 h / Heating
View Scheme
参考文献
Grotjahn; Vollhardt
Synthesis, 1993 , # 6 p. 579 - 605
反应条件
1: NH2OH*HCl, pyridine / ethanol / 36 h / 25 °C
2: 1,2-dimethoxy-ethane / 120 h / Heating
View Scheme
参考文献
Grotjahn; Vollhardt
Synthesis, 1993 , # 6 p. 579 - 605
反应条件
1: 80 percent / 5 percent aq. KOH / tetrahydrofuran; methanol / 3.8 h
2: 1,2-dimethoxy-ethane / 120 h / Heating
View Scheme
参考文献
Grotjahn; Vollhardt
Synthesis, 1993 , # 6 p. 579 - 605
