反应条件
1: 93 percent / 2percent NH3 in MeOH
2: 86 percent / K2CO3 / acetone / Heating
3: 79 percent / LiAlH4 / tetrahydrofuran / 1 h / Heating
4: 93 percent / NaIO4 / methanol; H2O / 1.5 h / 0 °C
5: 1) n-BuLi / 1) THF, hexane, -78 deg C, 15 min, 2) THF, hexane, -78 deg C, 30 min
6: 1) SOCl2, pyridine, 2) LiAlH4 / 1) THF, -10 deg C, 45 min, 2) THF, RT, 15 min then reflux, 30 min
View Scheme
参考文献
Czarnocki; Maclean; Szarek
Canadian Journal of Chemistry, 1986 , vol. 64, # 11 p. 2205 - 2210
