N-乙基-4-甲基-苯甲酰胺合成路线 （共 17 条）
反应条件
1,1,3,3-tetramethyldisiloxane; (μ3,η2,η3,η5-acenaphthylene)Ru(CO)7 in ethylene glycol dimethyl ether T=60°C; 12 h;
参考文献
Hanada, Shiori; Ishida, Toshiki; Motoyama, Yukihiro; Nagashima, Hideo
Journal of Organic Chemistry, 2007 , vol. 72, # 20 p. 7551 - 7559
反应条件
sodium hydride in tetrahydrofuran 1 h; Heating;
参考文献
Schmidt, Axel M.; Eilbracht, Peter
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 12 p. 2333 - 2343
反应条件
sodium hydroxide; potassium chloride; water T=100°C; other primary, secondary, and tertiary toluamides; hydrolysis and oxygen exchange rate constants; Product distributionRate constantMechanism;
参考文献
Slebocka-Tilk; Bennet; Keillor; Brown; Guthrie, J. Peter; Jodhan
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8507 - 8514
反应条件
sodium hydroxide; potassium chloride; water T=100°C; other primary, secondary, and tertiary toluamides; hydrolysis and oxygen exchange rate constants; Product distributionRate constantMechanism;
参考文献
Slebocka-Tilk; Bennet; Keillor; Brown; Guthrie, J. Peter; Jodhan
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8507 - 8514
反应条件
triethylamine in diethyl ether; water
参考文献
Hanada, Shiori; Tsutsumi, Emi; Motoyama, Yukihiro; Nagashima, Hideo
Journal of the American Chemical Society, 2009 , vol. 131, # 41 p. 15032 - 15040
反应条件
iodine; sodium hydroxide in water
T=60°C; 4 h;
参考文献
Ding, Jiaoyang; Cao, Liping; Wang, Jungang; Xue, Weijian; Zhu, Yanping; Wu, Anxin
Journal of Chemical Research, 2011 , vol. 35, # 5 p. 298 - 301
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 15 h; Inert atmosphere;
参考文献
Kitching, Matthew O.; Hurst, Timothy E.; Snieckus, Victor
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2925 - 2929
反应条件
1: 1.) Et3N / 1.) CH2Cl2, 25 deg C
2: Heating
View Scheme
参考文献
Wakselman, M.; Acher, F.
Tetrahedron Letters, 1980 , vol. 21, p. 2705 - 2708
反应条件
aluminum oxide
T=440 - 450°C;
参考文献
Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1920 , vol. 170, p. 813,815
Annales de Chimie (Cachan, France), 1868 , vol. <4> 13, p. 224,226
反应条件
NaOD; potassium chloride; water-d2
T=100°C; other amidines; Rate constantProduct distributionMechanism;
参考文献
Slebocka-Tilk; Bennet; Keillor; Brown; Guthrie, J. Peter; Jodhan
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8507 - 8514
