1-甲基氮杂环丁-2-酮合成路线 (共 14 条)
反应条件
in diethyl ether 1.5 h; Ambient temperature;
参考文献
Abboud; Canada; Homan; Notario; Cativiela; De Diaz Villegas; Bordeje; Mo; Yantez
Journal of the American Chemical Society, 1992 , vol. 114, # 12 p. 4728 - 4736
反应条件
diethyl ether anschliessend Behandeln mit wss.Ammoniumchlorid-Loesung;
参考文献
Holley; Holley
Journal of the American Chemical Society, 1949 , vol. 71, p. 2129
反应条件
in methanol T=-196°C; Irradiation;
参考文献
Tomioka, Hideo; Kondo, Masato; Izawa, Yasuji
Journal of Organic Chemistry, 1981 , vol. 46, p. 1090 - 1094
反应条件
bis(2-pyridinyl)-disulfide; triphenylphosphine in acetonitrile 5 h; Heating;
参考文献
Hanai, Kazuhiko; Maki, Yoshifumi; Kuwae, Akio
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1986 , vol. 42, # 8 p. 861 - 868
反应条件
T=150 - 170°C; Wolff Rearrangement; P=562.556 Torr; Inert atmosphere;
参考文献
Wentrup, Curt; Bibas, Herve; Kuhn, Arvid; Mitschke, Ullrich; McMills, Mark C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10705 - 10717
参考文献
Tomioka, Hideo; Kondo, Masato; Izawa, Yasuji
Journal of Organic Chemistry, 1981 , vol. 46, p. 1090 - 1094
反应条件
T=-265.16°C; Wolff Rearrangement; Photolysis;
参考文献
Wentrup, Curt; Bibas, Herve; Kuhn, Arvid; Mitschke, Ullrich; McMills, Mark C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10705 - 10717
反应条件
T=-266.16°C; Wolff Rearrangement; Photolysis;
参考文献
Wentrup, Curt; Bibas, Herve; Kuhn, Arvid; Mitschke, Ullrich; McMills, Mark C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10705 - 10717
参考文献
Holley; Holley
Journal of the American Chemical Society, 1949 , vol. 71, p. 2129
参考文献
Tomioka, Hideo; Kondo, Masato; Izawa, Yasuji
Journal of Organic Chemistry, 1981 , vol. 46, p. 1090 - 1094