2-(哌啶硫代)苯并噻唑合成路线 （共 15 条）
参考文献
Torii,S. et al.
Journal of Organic Chemistry, 1978 , vol. 43, p. 3223 - 3227
参考文献
I.G. Farbenind.
Patent: DE615580 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 22, p. 1752
Full Text Show Details
I.G. Farbenind.
Patent: US2045888 , 1934 ;
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C 2: Porcine pancreatic lipase type II / tert-butyl methyl ether; toluene / 2 h / 20 °C / pH 7.5 / aq. phosphate buffer; Enzymatic reaction 3: acetonitrile / 5 h / 20 °C View Scheme
参考文献
Du, Zhenjun; Kawatani, Toshihiro; Kataoka, Kazuhide; Omatsu, Rikiya; Nokami, Junzo
Tetrahedron, 2012 , vol. 68, # 11 p. 2471 - 2480
反应条件
1: potassium carbonate / acetone / 3 h / 20 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C 3: Porcine pancreatic lipase type II / tert-butyl methyl ether; toluene / 2 h / 20 °C / pH 7.5 / aq. phosphate buffer; Enzymatic reaction 4: acetonitrile / 5 h / 20 °C View Scheme
参考文献
Du, Zhenjun; Kawatani, Toshihiro; Kataoka, Kazuhide; Omatsu, Rikiya; Nokami, Junzo
Tetrahedron, 2012 , vol. 68, # 11 p. 2471 - 2480
反应条件
1: Porcine pancreatic lipase type II / tert-butyl methyl ether; toluene / 2 h / 20 °C / pH 7.5 / aq. phosphate buffer; Enzymatic reaction 2: acetonitrile / 5 h / 20 °C View Scheme
参考文献
Du, Zhenjun; Kawatani, Toshihiro; Kataoka, Kazuhide; Omatsu, Rikiya; Nokami, Junzo
Tetrahedron, 2012 , vol. 68, # 11 p. 2471 - 2480
反应条件
in acetonitrile T=20°C; sulfinyl-Knoevenagel reaction; 5 h; optical yield given as percent eeenantioselective reaction;
参考文献
Du, Zhenjun; Kawatani, Toshihiro; Kataoka, Kazuhide; Omatsu, Rikiya; Nokami, Junzo
Tetrahedron, 2012 , vol. 68, # 11 p. 2471 - 2480
参考文献
I.G. Farbenind.
Patent: DE586351 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 2020
参考文献
U.S. Rubber Co.
Patent: US2382793 , 1943 ;
参考文献
Monsanto Chem. Co.
Patent: US2368515 , 1940 ;
Full Text Show Details
Blake
Journal of the American Chemical Society, 1943 , vol. 65, p. 1267
参考文献
Chemistry Letters, , p. 695 - 698
