4-氯-N-甲基甲酰苯胺合成路线 （共 21 条）
反应条件
TEMPO; oxygen in acetonitrile T=50°C; P=760.051 Torr; 13 h;
参考文献
Song, Ren-Jie; Liu, Yu; Hu, Rui-Xiang; Liu, Yan-Yun; Wu, Ji-Cheng; Yang, Xu-Heng; Li, Jin-Heng
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1467 - 1473
反应条件
copper(l) iodide; cesium fluoride; N-methyl-2-(methylamino)ethylamine in tetrahydrofuran T=25°C; 18 - 24 h; Inert atmosphere;
参考文献
Phillips, Dean P.; Zhu, Xue-Feng; Lau, Thomas L.; He, Xiaohui; Yang, Kunyong; Liu, Hong
Tetrahedron Letters, 2009 , vol. 50, # 52 p. 7293 - 7296
反应条件
hydrogenchloride; zinc in water T=70°C; 3 h; Neat (no solvent);
参考文献
Kim, Joong-Gon; Jang, Doo Ok
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 10 p. 2989 - 2991
反应条件
potassium fluoride on basic alumina in acetonitrile 3 h; Heating;
参考文献
Mihara, Masatoshi; Ishino, Yoshio; Minakata, Satoshi; Komatsu, Mitsuo
Synthesis, 2003 , # 15 p. 2317 - 2320
反应条件
oxygen in acetonitrile T=60°C; 20 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
Benzoyl cyanide; oxygen; iron(III) chloride in acetonitrile T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298
反应条件
oxygen; iron(III) chloride in acetonitrile T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298
反应条件
oxygen; copper(l) chloride in acetonitrile T=30°C; P=760 Torr; 20 h;
参考文献
Murata, Satoru; Suzuki, Kaoru; Tamatani, Akira; Miura, Masahiro; Nomura, Masakatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1387 - 1392
反应条件
sulfuric acid Heating;
参考文献
Meth-Cohn, Otto; Taylor, David L.
Tetrahedron, 1995 , vol. 51, # 47 p. 12869 - 12882
反应条件
perchloryl fluoride in tetrahydrofuran T=0°C;
参考文献
Hiller, Achim; Patt, Joerg T.; Steinbach, Joerg
Journal of Organometallic Chemistry, 2006 , vol. 691, # 18 p. 3737 - 3742
