1,1,5-三氯-1-戊烯合成路线 （共 21 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran Heating;
参考文献
Zakharkin, L. I.; Anikina, E. V.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 12 p. 2217 - 2221
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 12 p. 2469 - 2474
反应条件
perchloric acid T=120°C;
参考文献
du Pont de Nemours and Co.
Patent: US2398430 , 1942 ;
反应条件
1: H2SO4 2: sulfuric acid View Scheme
参考文献
du Pont de Nemours and Co.
Patent: US2398430 , 1942 ;
参考文献
Kost,V.N. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 1835 - 1837
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , p. 1992 - 1995
反应条件
1: ethanol
2: 1.) Mg, 2.) aq. HCl / 1.) ether, reflux, 2 h, 2.) ether, reflux, 30 min
3: 78 percent
4: BuLi / diethyl ether; hexane; tetrahydrofuran / 2 h / 0 °C
5: 2.1 g / diethyl ether; hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 12 h / 20 °C
View Scheme
参考文献
Zakharkin, L.I.; Churilova, I.M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 11 p. 2412 - 2413
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 11 p. 2633 - 2635
反应条件
ammonia; sodium acetylene
T=-40°C;
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 846,849; engl. Ausg. S. 823, 825
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 1009,1013
Chem.Abstr., 1956 , # 1121
反应条件
1: ethanol
2: sodium; diethyl ether / anschliessendes Hydrolyse
View Scheme
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 1009,1013
Chem.Abstr., 1956 , # 1121
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 1009,1013
Chem.Abstr., 1956 , # 1121
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
Heating;
参考文献
Zakharkin, L. I.; Anikina, E. V.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 12 p. 2217 - 2221
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 12 p. 2469 - 2474
