1,1,5-三氯-1-戊烯合成路线 （共 21 条）
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone; iron(III) chloride in isopropyl alcohol Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
hexacarbonyl molybdenum in chloroform T=140°C; 5 h; other catalyst, solvent; Product distribution;
参考文献
Kuz'mina, N. A.; Blinova, N. V.; Chukovskaya, E. Ts.; Grechkina, E. M.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 5 p. 1032 - 1036
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 5 p. 1139 - 1142
反应条件
decacarbonyldimanganese (2); butane-1-thiol T=140°C; 4 h;
参考文献
Petrova, R. G.; Churkina, T. D.; Golikova, I. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 8 p. 1642 - 1646
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 8 p. 1816 - 1820
反应条件
pentacarbonyliron(0); butane-1-thiol T=140°C; 4 h;
参考文献
Petrova, R. G.; Churkina, T. D.; Golikova, I. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 8 p. 1642 - 1646
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 8 p. 1816 - 1820
反应条件
anhydrous diethylamine hydrochloride; 1,2-diphenyl-2-hydroxyethanone in isopropyl alcohol Further byproducts given;
参考文献
Moore,L.O.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2633 - 2635
反应条件
ammonia; platinum Hydrogenation;
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 657,660;engl.Ausg.S.585,587
反应条件
hexacarbonyl molybdenum in various solvent(s) T=140°C; 3 h; Product distribution;
参考文献
Blinova, N. V.; Kuz'mina, N. A.; Chukovskaya, E. Ts.; Vakhtagishvili, L. V.; Rusanov, A. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1609 - 1612
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 8 p. 1803 - 1806
参考文献
du Pont de Nemours and Co.
Patent: US2398430 , 1942 ;
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2410541 , 1942 ;
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 657,660;engl.Ausg.S.585,587
反应条件
1: sodium iodide; aqueous ethanol 2: 1,1,1,5-tetrachloro-pentane; Raney nickel; methanol / 75 °C / 73550.8 Torr / Hydrogenation 3: H2SO4 View Scheme
参考文献
Nessmajanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1954 , p. 34,38
Chem.Abstr., 1955 , # 6085
