2-氯-N,N-二甲基乙酰胺合成路线 （共 38 条）
反应条件
sodium hydride in diethyl ether
Ambient temperature;
参考文献
van der Stelt,C. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1973 , vol. 92, p. 493 - 512
参考文献
Marini-Bettolo; Cavalla
Gazzetta Chimica Italiana, 1954 , vol. 84, p. 896,905
反应条件
triethylamine in acetonitrile
参考文献
Ono Pharmaceutical Co., Ltd.
Patent: US4021472 A1, 1977 ;
反应条件
(i), (ii) H2S, benzene; Multistep reaction;
参考文献
Mathey,F. et al.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 2402 - 2410
参考文献
Boehme,H.; Krack,W.
Justus Liebigs Annalen der Chemie, 1977 , p. 1291 - 1295
参考文献
Green, James R.; Majewski, Marek; Snieckus, Victor
Canadian Journal of Chemistry, 2006 , vol. 84, # 10 p. 1397 - 1410
反应条件
methanol
T=40°C; 4 h; Inert atmosphere;
参考文献
Vidal, Thierry; Guglieri, Massimo; Jentzer, Olivier
Patent: US2012/302791 A1, 2012 ;
Location in patent: Page/Page column 24 ;
反应条件
trichlorophosphate
1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction;
参考文献
Croce, Piero Dalla; Rosa, Concetta La; Ritieni, Alberto
Synthesis, 1989 , # 10 p. 783 - 784
