N-(3-氨基丙基)-n-环己基-n-甲胺合成路线 (共 3 条)
反应条件
diethyl ether; ammonia; nickel T=125°C; P=73550.8 - 91938.4 Torr; Hydrogenation;
参考文献
Corse et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1911
反应条件
1: With sodium tris(acetoxy)borohydride T=20°C; 2: With methanol; ammonia
参考文献
GLAXO GROUP LIMITED
Patent: WO2007/138033 A1, 2007 ;
Location in patent: Page/Page column 29 ;
反应条件
1: trimethyl-benzyl-ammonium hydroxide 2: Raney nickel; diethyl ether; ammonia / 125 °C / 73550.8 - 91938.4 Torr / Hydrogenation View Scheme
参考文献
Corse et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1911