三甲基1,2,3-苯三甲酸合成路线 （共 18 条）
反应条件
in dichloromethane
T=20°C; P=11250900 Torr; 12 h;
参考文献
Revial, Gilbert; Blanchard, Mireille; d'Angelo, Jean
Tetrahedron Letters, 1983 , vol. 24, # 9 p. 899 - 902
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
24 h; Heating;
参考文献
Koike, Takeshi; Tanabe, Mituharu; Takeuchi, Naoki; Tobinaga, Seisho
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 2 p. 243 - 248
反应条件
sulfuric acid in 1,2-dichloro-ethane
参考文献
Hefelfinger,D.T.; Cram,D.J.
Journal of the American Chemical Society, 1971 , vol. 93, p. 4754 - 4767
参考文献
Ziegler, Thomas; Layh, Marcus; Effenberger, Franz
Chemische Berichte, 1987 , vol. 120, p. 1347 - 1356
反应条件
in xylene
2 h; Heating;
参考文献
Koike, Takeshi; Tanabe, Mituharu; Takeuchi, Naoki; Tobinaga, Seisho
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 2 p. 243 - 248
参考文献
Ziegler, Thomas; Layh, Marcus; Effenberger, Franz
Chemische Berichte, 1987 , vol. 120, p. 1347 - 1356
反应条件
dicobalt octacarbonyl in methanol
T=65°C; 95 h; P(CO): 2 kg/cm-2;
参考文献
Kazimura, Tsugunori; Kudo, Kiyoshi; Mori, Sadayuki; Sugita, Nobuyuki
Chemistry Letters, 1986 , p. 851 - 854
反应条件
1: 80 percent / NaOH, KMnO4 / H2O / 2 h / Heating
2: methanol; diethyl ether
View Scheme
参考文献
Capassso, Renato; Randazzo, Giacomino; Stipani, Italo; Zara, Vincenzo; Palmieri, Ferdinando
Gazzetta Chimica Italiana, 1989 , vol. 119, # 8 p. 449 - 452
反应条件
in xylene
40 h; Heating;
参考文献
Noguchi, Michihiko; Kakimoto, Shinji; Kajigaeshi, Shoji
Heterocycles, 1986 , vol. 24, # 3 p. 665 - 668
反应条件
in neat (no solvent)
T=63°C; 20 h; Product distributionMechanism;
参考文献
Noland, Wayland E.; Lee, Chang Kiu
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4573 - 4582
