4-甲基-1,2-苯二磺酰基二氯化物合成路线 (共 2 条)
反应条件
water; chlorine in dichloromethane; tert-butyl alcohol T=0 - 5°C; 1 h;
参考文献
Barbero, Margherita; Berto, Silvia; Cadamuro, Silvano; Daniele, Pier Giuseppe; Dughera, Stefano; Ghigo, Giovanni
Tetrahedron, 2013 , vol. 69, # 15 p. 3212 - 3217
反应条件
1: 1,4-dioxane; dichloromethane; 3-methyl-1-butanol / 1.75 h / 20 - 82 °C 2: chlorine; water / tert-butyl alcohol; dichloromethane / 1 h / 0 - 5 °C View Scheme
参考文献
Barbero, Margherita; Berto, Silvia; Cadamuro, Silvano; Daniele, Pier Giuseppe; Dughera, Stefano; Ghigo, Giovanni
Tetrahedron, 2013 , vol. 69, # 15 p. 3212 - 3217