(2E)-4-甲基-3-氧代-N-苯基-2-[(2H5)苯基亚甲基]戊酰胺合成路线 (共 3 条)
反应条件
1: 97 percent / toluene / 4 h / 80 °C 2: 15.26 g / β-alanine; glacial acetic acid / hexane / 25 h / Heating View Scheme
参考文献
Chen, Bang-Chi; Sundeen, Joseph E.; Guo, Peng; Bednarz, Mark S.; Hangeland, Jon J.; Ahmed, Syed Z.; Jemal, Mohammed
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 3 p. 261 - 270
反应条件
acetic acid; 3-aminopropionic acid in hexane Condensation; 25 h; Heating;
参考文献
Chen, Bang-Chi; Sundeen, Joseph E.; Guo, Peng; Bednarz, Mark S.; Hangeland, Jon J.; Ahmed, Syed Z.; Jemal, Mohammed
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 3 p. 261 - 270
反应条件
1: 4.7 g / 3-ethyl-5-(2-hydroxyethyl)-4-methylthiazolium bromide; triethylamine / ethanol / 21 h / 75 - 80 °C 2: 4.07 g / pivalic acid / tetrahydrofuran; toluene; heptane / 24 h / Heating View Scheme
参考文献
Chen, Bang-Chi; Sundeen, Joseph E.; Guo, Peng; Bednarz, Mark S.; Hangeland, Jon J.; Ahmed, Syed Z.; Jemal, Mohammed
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 3 p. 261 - 270