5-乙酰乙酰氨基苯并咪唑酮合成路线 (共 3 条)
反应条件
in acetonitrile T=100°C; 2 h;
参考文献
AGFA-GEVAERT
Patent: WO2007/6636 A2, 2007 ;
Location in patent: Page/Page column 40-41 ;
反应条件
1: anthranilic acid With hydrogenchloride in water 2: With sodium nitrite in water T=0°C; 0.5 h; 3: 5-Acetoacetyl-amino-benzimidazol-2-one With acetic acid; sodium hydroxide in water T=20°C; 6 h; Product distribution / selectivity;
参考文献
Xerox Corporation; National Research Council of Canada
Patent: EP2290012 A2, 2011 ;
Location in patent: Page/Page column 122 ;
反应条件
1: 5-Acetoacetyl-amino-benzimidazol-2-one With sodium hydroxide in water 2: benzenediazonium-2-carboxylate hydrochloride With sodium hydroxide; acetic acid in water Product distribution / selectivity;
参考文献
Xerox Corporation
Patent: US7503973 B1, 2009 ;
Location in patent: Page/Page column 20 ;