1: (S)-N-benzyl-α-methylbenzylamine With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: tert-butyl cinnamoate in tetrahydrofuran; hexane T=-78°C; 2 h; Inert atmosphere; 3: With water; ammonium chloride in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Davies, Stephen G.; Foster, Emma M.; McIntosh, Catherine R.; Roberts, Paul M.; Rosser, Timothy E.; Smith, Andrew D.; Thomson, James E.
Tetrahedron Asymmetry, 2011 , vol. 22, # 10 p. 1035 - 1050
in tetrahydrofuran T=-78°C; 2 h; Inert atmosphere; diastereoselective reaction;
参考文献
Davies, Stephen G.; Fletcher, Ai M.; Lee, James A.; Roberts, Paul M.; Souleymanou, Myriam Y.; Thomson, James E.; Zammit, Charlotte M.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 17 p. 2702 - 2728
Davies, Stephen G.; Garner, A. Christopher; Roberts, Paul M.; Smith, Andrew D.; Sweet, Miles J.; Thomson, James E.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 14 p. 2753 - 2768
