N,N,N’,N’-四甲基-L-酒石酰胺合成路线 （共 13 条）
反应条件
potassium hydroxide in methanol
参考文献
Seebach,D. et al.
Helvetica Chimica Acta, 1977 , vol. 60, p. 301 - 325
反应条件
in tetrahydrofuran 120 h; Ambient temperature;
参考文献
Gawronski, Jacek; Gawronska, Krystyna; Skowronek, Pawel; Rychlewska, Urszula; Warzajtis, Beata; Rychlewski, Jacek; Hoffmann, Marcin; Szarecka, Agnieszka
Tetrahedron, 1997 , vol. 53, # 17 p. 6113 - 6144
反应条件
(i) (esterification), (ii) /BRN= 605257/, MeOH; Multistep reaction;
参考文献
Seebach,D. et al.
Angewandte Chemie, 1969 , vol. 81, p. 1002 - 1003
反应条件
sodium hydride in tetrahydrofuran
参考文献
Seebach,D. et al.
Helvetica Chimica Acta, 1977 , vol. 60, p. 301 - 325
反应条件
(i) TlOEt, benzene, (ii) /BRN= 969135/, MeCN; Multistep reaction;
参考文献
Kalinowski, Hans-Otto; Crass, Gerhard; Seebach, Dieter
Chemische Berichte, 1981 , vol. 114, # 2 p. 477 - 487
反应条件
1: <PhCH2NEt3>Cl, aq. NaOH 2: LiAlH4 View Scheme
参考文献
Seebach,D. et al.
Helvetica Chimica Acta, 1977 , vol. 60, p. 301 - 325
反应条件
1: NaH / tetrahydrofuran
2: LiAlH4 / tetrahydrofuran
View Scheme
参考文献
Seebach,D. et al.
Helvetica Chimica Acta, 1977 , vol. 60, p. 301 - 325
反应条件
sodium hydride in N,N-dimethyl-formamide
T=80°C; 8 h;
参考文献
Anantanarayan, A.; Carmicheal, V.A.; Dutton, P.J.; Fyles, T.M.; Pitre, M.J.
Synthetic Communications, 1986 , vol. 16, # 14 p. 1771 - 1776
反应条件
thallium ethylate in N,N-dimethyl-formamide
参考文献
Anantanarayan, A.; Carmicheal, V.A.; Dutton, P.J.; Fyles, T.M.; Pitre, M.J.
Synthetic Communications, 1986 , vol. 16, # 14 p. 1771 - 1776
反应条件
thallium ethylate
1.) DMF, rt, 30 min, 2.) rt, 1 h; from rt to 70 deg C, 1 h; 70 deg C, 8 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Behr, Jean-Paul; Girodeau, Jean-Marc; Hayward, Rodney C.; Lehn, Jean-Marie; Sauvage, Jean-Pierre
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 2096 - 2111
