N-苄氧羰基-L-谷氨酰胺合成路线 （共 50 条）
反应条件
1: With sodium hydrogencarbonate in water; toluene T=20°C; Inert atmosphere; 2: With hydrogenchloride in water
参考文献
PERSCITUS BIOSCIENCES, LLC
Patent: WO2008/119032 A1, 2008 ;
Location in patent: Page/Page column 32 ;
反应条件
water; triethylamine in 1,4-dioxane T=20°C; Acylation; 1 h;
参考文献
Yasuhara, Tomohisa; Nagaoka, Yasuo; Tomioka, Kiyoshi
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2233 - 2234
反应条件
triethylamine in water; acetone Ambient temperature;
参考文献
Kunieda, Takehisa; Higuchi, Tsunehiko; Abe, Yoshihiro; Hirobe, Masaaki
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 6 p. 2174 - 2181
反应条件
1: 83 percent / pyridine / Ambient temperature 2: 81 percent / Et3N / acetone; H2O / Ambient temperature View Scheme
参考文献
Yasuhara, Tomohisa; Nagaoka, Yasuo; Tomioka, Kiyoshi
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2233 - 2234
参考文献
Bergmann; Zervas
Chemische Berichte, 1932 , vol. 65, p. 1192,1198
Full Text Show Details
Melville
Biochemical Journal, 1935 , vol. 29, p. 179,182
参考文献
I.G. Farbenind.
Patent: DE624230 , 1934 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 22, p. 188
反应条件
hydrogenchloride; sodium nitrite Umsetzung des gebildeten Azids mit NH3 in Aether;
参考文献
I.G. Farbenind.
Patent: DE624230 , 1934 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 22, p. 188
参考文献
Gibian,H.; Klieger,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 640, p. 145 - 156
反应条件
1: toluene / anfangs unter Kuehlung 2: aqueous NaHCO3 View Scheme
参考文献
Bergmann; Zervas
Chemische Berichte, 1932 , vol. 65, p. 1192,1198
参考文献
Voelter,W. et al.
Monatshefte fuer Chemie, 1974 , vol. 105, p. 1110 - 1135
