1,3,5-三甲基-1H-吡唑-4-甲醛合成路线 （共 6 条）
反应条件
trichlorophosphate T=90 - 120°C; Vilsmeier-Haak formylation; 1 h;
参考文献
Attaryan; Antanosyan; Panosyan; Asratyan; Matsoyan
Russian Journal of General Chemistry, 2006 , vol. 76, # 11 p. 1817 - 1819
反应条件
iodine in toluene 0.5 h; Heating;
参考文献
Henn, Lothar; Hickey, Deirde M. B.; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2189 - 2197
反应条件
in xylene 0.333333 h; Heating;
参考文献
Henn, Lothar; Hickey, Deirde M. B.; Moody, Christopher J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2189 - 2197
反应条件
1: potassium hydroxide; hydroxylamine hydrochloride / ethanol; water 2: acetic anhydride / 1 h / |Reflux View Scheme
参考文献
Attaryan; Sahakyan; Tamazyan; Ayvazyan; Asratyan
Russian Journal of General Chemistry, 2012 , vol. 82, # 10 p. 1720 - 1723
Zh. Obshch. Khim., 2012 , vol. 82, # 10 p. 1716 - 1719,4
反应条件
sodium hydroxide in water T=70°C; Electrochemical reaction;
参考文献
Russian Chemical Bulletin, , vol. 61, # 6 p. 1148 - 1153
Izv. Akad. Nauk, Ser. Khim., , vol. 61, # 6 p. 1139 - 1143,5
反应条件
sodium tetrahydroborate; N-benzyl-N,N,N-triethylammonium chloride in water T=20°C; 3 h;
参考文献
Attaryan; Gevorkyan; Antanosyan; Martirosyan; Panosyan; Matsoyan
Russian Journal of General Chemistry, 2005 , vol. 75, # 9 p. 1500 - 1501
