(2E)-3-环己基-2-丙烯酸甲酯合成路线 (共 25 条)
反应条件
n-butyllithium; sulfuric acid
1.) hexane, THF, -78 deg C to -20 deg C;
参考文献
Smithers, Roger H.
Synthetic Communications, 1985 , vol. 15, # 2 p. 81 - 86
反应条件
benzophenone
4.5 h; Irradiation;
参考文献
Doohan, Roisin A.; Hannan, John J.; Geraghty, Niall W.A.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 5 p. 942 - 952
反应条件
sodium hydride; sodium iodide in tetrahydrofuran
T=-78°C; Horner-Wadsworth-Emmons olefination; 2 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Pihko, Petri M.; Salo, Taina M.
Tetrahedron Letters, 2003 , vol. 44, # 23 p. 4361 - 4364
反应条件
T=400°C; 0.0166667 h; Yield given. Yields of byproduct given;
参考文献
Metzger, Juergen O.; Klenke, Kurt; Hartmanns, Joerg; Eisermann, Doris
Chemische Berichte, 1986 , vol. 119, # 2 p. 508 - 513
反应条件
T=400°C; 0.0166667 h; Yield given. Yields of byproduct given;
参考文献
Metzger, Juergen O.; Klenke, Kurt; Hartmanns, Joerg; Eisermann, Doris
Chemische Berichte, 1986 , vol. 119, # 2 p. 508 - 513