2,5-双(三氟甲基)-3,6-二氧杂十一氟代壬酰氟合成路线 （共 33 条）
反应条件
potassium fluoride T=140°C; 1 h;
参考文献
ASAHI GLASS COMPANY LTD.
Patent: EP1574497 A1, 2005 ;
Location in patent: Page/Page column 23 ;
反应条件
potassium fluoride T=200°C; 2 h; Autoclave;
参考文献
Okazoe, Takashi; Watanabe, Kunio; Itoh, Masahiro; Shirakawa, Daisuke; Takagi, Hirokazu; Kawahara, Kengo; Tatematsu, Shin
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 8 p. 1611 - 1616
反应条件
1: 2,3,3,3-tetrafluoro-2-(pentafluorophenoxy)propionyl fluoride With potassium fluoride in 1.4-dicyano 1-butene; bis [2-(2-methoxyethoxy)ethyl] ether 0.5 h; 2: hexafluorocyclopropylene oxide in 1.4-dicyano 1-butene; bis [2-(2-methoxyethoxy)ethyl] ether T=25 - 29°C; Product distribution / selectivity;
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: EP939752 B1, 2005 ;
Location in patent: Page/Page column 5-6 ;
反应条件
potassium fluoride in diethylene glycol dimethyl ether 24 h; Ambient temperature; Further byproducts given;
参考文献
Ishikawa, Nobuo; Sasabe, Mikio
Journal of Fluorine Chemistry, 1984 , vol. 25, p. 241 - 254
反应条件
cesium fluoride in various solvent(s)
参考文献
Paleta, Oldrich; Palecek, Jiri; Michalek, Jiri
Journal of Fluorine Chemistry, 2002 , vol. 114, # 1 p. 51 - 53
反应条件
potassium fluoride in diethylene glycol dimethyl ether 24 h; Ambient temperature; Further byproducts given;
参考文献
Ishikawa, Nobuo; Sasabe, Mikio
Journal of Fluorine Chemistry, 1984 , vol. 25, p. 241 - 254
反应条件
potassium fluoride; ethyl fluorooxolate in diethylene glycol dimethyl ether 14 h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Paleta, Oldrich; Cirkva, Vladimir; Kvicala, Jaroslav
Journal of Fluorine Chemistry, 1996 , vol. 80, # 2 p. 125 - 134
反应条件
Cu2Cl2 in acetonitrile oligomerization; Title compound not separated from byproducts;
参考文献
Yuminov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 12 p. 1715 - 1720
反应条件
potassium fluoride T=117 - 120°C; 3 h; Pyrolysis;
参考文献
ASAHI GLASS COMPANY, LIMITED
Patent: WO2005/123650 A1, 2005 ;
Location in patent: Page/Page column 21 ;
反应条件
T=20°C; 24 h; Yield given;
参考文献
Yuminov, V. S.
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 3 p. 300 - 302
Zhurnal Organicheskoi Khimii, 1997 , vol. 33, # 3 p. 344 - 347
