N-(2-氯乙基)苯甲酰胺合成路线 （共 47 条）
反应条件
1: n-buthyl-lithium, lithium naphthalenide / tetrahydrofuran; diethyl ether / 4 h / -78 °C
2: H2O / -78 - 20 °C
3: 73 percent / H2SO4 / ethanol; dioxane / 12 h / Heating
View Scheme
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Tetrahedron, 1989 , vol. 45, # 7 p. 2183 - 2192
反应条件
Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Tetrahedron Letters, 1992 , vol. 33, # 41 p. 6183 - 6186
反应条件
1: n-buthyl-lithium, lithium naphthalenide / tetrahydrofuran; diethyl ether / 4 h / -78 °C
2: H2O / -78 - 20 °C
View Scheme
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Tetrahedron, 1989 , vol. 45, # 7 p. 2183 - 2192
反应条件
n-butyllithium; naphthalenyllithium
1.) THF, ether, -78 deg C, 20 min 2.) THF, 5 h, -78 deg C; 3. overnight, 20 deg C; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Tetrahedron Letters, 1988 , vol. 29, # 23 p. 2859 - 2860
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane
1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Barluenga, Jose; Montserrat, Javier M.; Florez, Josefa
Journal of Organic Chemistry, 1993 , vol. 58, # 22 p. 5976 - 5980
反应条件
n-butyllithium; water; naphthalenyllithium
1.) THF, ether, -78 deg C, 20 min 2.) THF, 5 h, -78 deg C; 3.) 20 deg C; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Foubelo, Francisco; Fananas, Francisco J.; Yus, Miguel
Tetrahedron, 1989 , vol. 45, # 7 p. 2183 - 2192
反应条件
sodium tetrahydroborate in ethanol
Heating;
参考文献
Singh; Sooriyakumar; Kadarkaraisamy; Drake; Hursthouse; Light; Butcher
Journal of Chemical Research - Part S, 2001 , # 8 p. 339 - 341
