三环己基膦与二硫化碳(1:1)化合物合成路线 (共 2 条)
反应条件
1: cyclohexyl monochloride With magnesium; ethylene dibromide in diethyl ether T=41°C; 2 h; Heating / reflux; 2: With phosphorus trichoride in diethyl ether; tert-butyl methyl ether T=-17 - 20°C; Heating / reflux; 3: carbon disulfide in diethyl ether; tert-butyl methyl ether Product distribution / selectivity;
参考文献
Dynamit Nobel GmbH Explosivstoff- und Systemtechnik
Patent: EP2019107 A1, 2009 ;
Location in patent: Page/Page column 6 ;
反应条件
in ethanol T=78 - 79°C; Product distribution / selectivity;
参考文献
Dynamit Nobel GmbH Explosivstoff- und Systemtechnik
Patent: EP2019107 A1, 2009 ;
Location in patent: Page/Page column 6; 9-10 ;