4-溴-1,2-亚甲二氧基苯合成路线 （共 128 条）
反应条件
ammonium cerium(IV) nitrate; lithium bromide in acetonitrile T=20°C; 2 h;
参考文献
Roy, Subhas Chandra; Guin, Chandrani; Rana, Kalyan Kumar; Maiti, Gourhari
Tetrahedron Letters, 2001 , vol. 42, # 39 p. 6941 - 6942
反应条件
[Cp*Ru(CH3CN)3][SO3CF3]; lithium bromide T=100°C; 12 h; Inert atmosphere;
参考文献
Imazaki, Yusuke; Shirakawa, Eiji; Ueno, Ryota; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 36 p. 14760 - 14763
反应条件
tert-butyldimethylsilyl chloride in tetrachloromethane T=70°C; 4.5 h;
参考文献
Gesson, Jean-Pierre; Mondon, Martine; Pokrovska, Natacha
Synlett, 1997 , # 12 p. 1395 - 1396
参考文献
US2014/128392 A1, ;
Page/Page column ;
反应条件
1: 60 percent / NaIO4 2: 70 percent / TBDMSCl / CCl4 / 4.5 h / 70 °C View Scheme
参考文献
Gesson, Jean-Pierre; Mondon, Martine; Pokrovska, Natacha
Synlett, 1997 , # 12 p. 1395 - 1396
反应条件
chloro-trimethyl-silane in toluene Ambient temperature;
参考文献
Gesson, Jean-Pierre; Mondon, Martine; Pokrovska, Natacha
Synlett, 1997 , # 12 p. 1395 - 1396
参考文献
Gensler; Stouffer
Journal of Organic Chemistry, 1958 , vol. 23, p. 908
反应条件
palladium diacetate; triethylamine; triphenylphosphine T=110°C; 4 h;
参考文献
Dashkina, L. R.; Kulak, A. N.; Kasatkin, A. N.; Zorin, V. V.; Rakhmankulov, D. L.; Beletskaya, I. P.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 3.1 p. 422 - 426
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 3 p. 393 - 396
反应条件
1: 1.) n-BuLi / 1.) Et2O, 0 deg C 2: NaBH4 / ethanol / -22 °C View Scheme
参考文献
Schkeryantz, Jeffrey M.; Pearson, William H.
Tetrahedron, 1996 , vol. 52, # 9 p. 3107 - 3116
参考文献
Bristol-Myers Squibb
Patent: US5391570 A1, 1995 ;
US 5391570 A
