5,10,15,20-四苯基-21H,23H-卟吩二氯化锡(IV)合成路线 (共 2 条)
反应条件
air in pyridine Sn(II)-contg. compd. (1.72 mmol) was added to a soln. of a ligand (0.77 mmol) in pyridine; the mixt. was heated at reflux for 3 h; water was added; the ppt. was filtered, washed with water and air dried;
参考文献
Crossley; Thordarson; Wu
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2294 - 2302
反应条件
according to: A. D. Adler, F. R. Longo, F. Kampas, J. Kim, J. Inorg. Nuclear Chem. 32 (1970) 2443; chromy. (twice, Al2O3, chloroform);
参考文献
Lomova, T. N.; Berezin, B. D.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1979 , vol. 24, p. 874 - 878
Zhurnal Neorganicheskoi Khimii, 1979 , vol. 24, p. 1574 - 1581