(三-2-丙烯-1-基硅烷基)-苯合成路线 (共 61 条)
反应条件
in diethyl ether T=20°C;
参考文献
Andres, Roman; De Jesus, Ernesto; De La Mata, F. Javier; Flores, Juan C.; Gomez, Rafael
European Journal of Inorganic Chemistry, 2005 , # 18 p. 3742 - 3749
反应条件
in tetrahydrofuran T=-0.16 - 4.84°C; 24 h;
参考文献
Zhang, Daohong; Liang, Enbin; Li, Tingcheng; Chen, Sufang; Zhang, Junheng; Cheng, Xinjian; Zhou, Jiliang; Zhang, Aiqing
RSC Advances, 2013 , vol. 3, # 24 p. 9522 - 9529
反应条件
zinc in tetrahydrofuran 0.166667 h; Inert atmosphereSonication;
参考文献
Ramesh, Remya; Reddy, D. Srinivasa
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 24 p. 4093 - 4097
反应条件
in tetrahydrofuran T=20°C; 1 h;
参考文献
Li, Zhifang; Cao, Xiaojun; Lai, Guoqiao; Liu, Jinhua; Ni, Yong; Wu, Jirong; Qiu, Huayu
Journal of Organometallic Chemistry, 2006 , vol. 691, # 22 p. 4740 - 4746
反应条件
in diethyl ether T=35°C; 1 h;
参考文献
Boudin, Alain; Cerveau, Genevieve; Chuit, Claude; Corriu, Robert J. P.
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 1 p. 101 - 106
反应条件
1: 3-chloroprop-1-ene With magnesium 2: phenyl-trichloro-silane
参考文献
Zhang, Daohong; Liang, Enbin; Li, Tingcheng; Chen, Sufang; Zhang, Junheng; Cheng, Xinjian; Zhou, Jiliang; Zhang, Aiqing
RSC Advances, 2013 , vol. 3, # 9 p. 3095 - 3102
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: 4-chloro-2-fluoro-1-methoxybenzene With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: PTAS With tetrabutyl ammonium fluoride in water; dimethyl sulfoxide T=20°C; 1 h; 2: 4-bromobenzyl-alcohol With tri-cyclo-hexyl-phosphine; palladium dichloride in water; dimethyl sulfoxide T=80°C; 4 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
反应条件
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: 1-chloro-2-fluorobenzene With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Nakao, Yoshiaki; Hiyama, Tamejiro
Chemistry Letters, 2004 , vol. 33, # 5 p. 632 - 633
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide T=80°C; 4 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727