2-乙氧基-N,N-二甲基乙胺合成路线 (共 16 条)
反应条件
1: With hydrogen; nickel in methanol T=90°C; P=30003 Torr; 6 h; 2: With hydrogenchloride in methanol; water T=0°C; 3: With sodium hydroxide in water T=0°C;
参考文献
KOEI CHEMICAL CO., LTD.
Patent: EP1595863 A1, 2005 ;
Location in patent: Page/Page column 15-16 ;
反应条件
hydrogen; palladium on aluminum oxide T=100 - 130°C; P=7500.75 - 18751.9 Torr; Neat (no solvent);
参考文献
SASOL GERMANY GMBH
Patent: WO2004/24671 A1, 2004 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium in diethyl ether T=0°C; 3 h;
参考文献
Dubowchik, Gene M.; Gottschall, David W.; Grossman, Michael J.; Norton, Robert L.; Yoder, Claude H.
Journal of the American Chemical Society, 1982 , vol. 104, # 15 p. 4211 - 4214
反应条件
Cs-P-Si mixed-oxide T=300°C; P=61504.9 Torr;
参考文献
Oku, Tomoharu; Ikariya, Takao
Angewandte Chemie - International Edition, 2002 , vol. 41, # 18 p. 3476 - 3479
反应条件
2 h; Ambient temperature;
参考文献
Domer; Chihal; Charles; Koch
Journal of Medicinal Chemistry, 1980 , vol. 23, # 5 p. 541 - 545
参考文献
Grail et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1313
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Takahashi; Ohsawa
Yakugaku Zasshi, 1944 , vol. 64, # 7 p. 10
Chem.Abstr., 1951 , p. 8529
参考文献
Haarstad; Domer; Chihal; Rege; Charles
Journal of Medicinal Chemistry, 1976 , vol. 19, # 6 p. 760 - 763
参考文献
Knorr
Chemische Berichte, 1904 , vol. 37, p. 3501
参考文献
Knorr
Chemische Berichte, 1904 , vol. 37, p. 3501
反应条件
T=150 - 160°C; im Rohr; aceto-β-methylmorphimethine;
参考文献
Knorr; Hoerlein; Staubach
Chemische Berichte, 1909 , vol. 42, p. 3521