1,3,5-三氯-2,4,6-硝基苯合成路线 （共 22 条）
反应条件
sulfuric acid; potassium nitrate T=80 - 130°C; 18 h;
参考文献
Tao, Zhi-Gang; Zhao, Xin; Jiang, Xi-Kui; Li, Zhan-Ting
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1840 - 1842
反应条件
sulfuric acid; nitric acid
参考文献
Koninklijke Philips Electronics N.V.
Patent: EP1019401 B1, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
sulfuric acid; nitric acid T=150°C; 3.5 h;
参考文献
Mehilal; Salunke; Agrawal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 3 p. 604 - 607
反应条件
1: 100.6 percent / nitric acid / H2SO4 / 25 - 75 °C 2: nitric acid / various solvent(s) / 150 °C / acidity dependence of formation of TetCDNB View Scheme
参考文献
Moodie, Roy B.; Payne, Malcolm A.; Schofield, Kenneth
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1457 - 1464
反应条件
nitric acid in various solvent(s) T=150°C;
参考文献
Moodie, Roy B.; Payne, Malcolm A.; Schofield, Kenneth
Journal of the Chemical Society, Chemical Communications, 1983 , # 5 p. 233 - 234
反应条件
sulfuric acid; nitric acid
参考文献
Jackson; Carlton
American Chemical Journal, 1904 , vol. 31, p. 366
Chemische Berichte, 1902 , vol. 35, p. 3855
反应条件
T=80 - 90°C; Eintragen von HNO3 in das erkaltete Reatkionsgemisch und anschliessendes Erhitzen auf 140-150grad;
参考文献
Turek
Chimie et Industrie (Paris), 1931 , vol. 26, p. 781,785 Anm.
Full Text Show Details
Backer; van der Baan
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 1161,1165
参考文献
Wolff; Zietsch; Nuber; Gredel; Speiser; Wuerde
Journal of Organic Chemistry, 2001 , vol. 66, # 8 p. 2769 - 2777
反应条件
byproducts: CNCl, C2Cl6, CCl4; 340 to 350°C, pressure: 1 atm, in a bomb at higher pressure ( 10 to 15 atm He ) cooled explosion mixt. to room temp. contains more vol.-percent COCl2;
参考文献
Schubert, H.; Volk, F.
Brennstoff-Chemie, 1967 , vol. 48, p. 110 - 114
Full Text Show Details
Gmelin Handbook: C: MVol.D3, 2.2.2.7, page 63 - 65
反应条件
methanol; sodium azide
参考文献
Turek
Chimie et Industrie (Paris), 1931 , vol. 26, p. 781,785 Anm.
Full Text Show Details
Turk
Patent: DE498050 , 1927 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 655
