1,4-双(氯二氟甲基)苯合成路线 （共 6 条）
反应条件
chlorine T=60°C; P=760.051 Torr; 1.66667 h; Irradiation; TimeTemperatureReagent/catalyst;
参考文献
Chung-shan Institute of Science and Technology. Armaments Bureau. M.N.D.; Yuan-Shin Materials Technology Corp.; LIN, Chun-Hsu; Yin, Hung-Cheng; Sun, Chien-Yi; Yin, Yung-Yu; Chou, Chuan-Yu
Patent: US2013/116482 A1, 2013 ;
Location in patent: Paragraph 0036; 0037; 0038 ;
反应条件
chlorine in tetrachloromethane
参考文献
Union Carbide Chemicals and Plastics Technology Corporation
Patent: US5210341 A1, 1993 ;
反应条件
hydrogen fluoride in 1,2-dichloro-ethane T=45°C; P=2280.15 Torr; 10 h;
参考文献
Dolbier Jr., William R.; Duan, Jian-Xin; Rong, Xiao X.
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1091 - 1093
反应条件
potassium iodide; zinc in N,N-dimethyl acetamide T=120 - 142°C; 6 h; Catalytic behavior; Reagent/catalystSolventTemperature;
参考文献
LIN, Chun-Hsu; SUN, Chien-Yi; YIN, Yung-Yu; LI, Chun-Shih; CHOU, Yo-Chun
Patent: US2014/11986 A1, 2014 ;
Location in patent: Paragraph 0024 ;
反应条件
zinc in N,N-dimethyl acetamide T=100°C; Substitution; 4 h;
参考文献
Organic Letters, , vol. 2, # 13 p. 1867 - 1869
反应条件
calcium chloride; zinc in N,N-dimethyl acetamide T=120 - 140°C; 4 h; Catalytic behavior; Reagent/catalyst;
参考文献
LIN, Chun-Hsu; SUN, Chien-Yi; YIN, Yung-Yu; LI, Chun-Shih; CHOU, Yo-Chun
Patent: US2014/11986 A1, 2014 ;
Location in patent: Paragraph 0048 ;
