(S)-(-)- α-甲基苄胺合成路线 （共 369 条）
反应条件
benzil
T=149.85°C; 0.5 h;
参考文献
Vazquez Garcia, Rosa A.; Bernes, Sylvain; Gutierrez Perez, Rene; Martinez Garcia, Marcos
Acta Crystallographica Section C: Crystal Structure Communications, 2002 , vol. 58, # 10 p. o619-o620
反应条件
1: 23 percent / acetonitrile / 2 h / Heating
2: 32 percent / LiAlH4 / diethyl ether / 4 h / Heating
View Scheme
参考文献
Potapov, V. M.; Gracheva, R. A.; Savina, S. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, p. 1902 - 1904
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 10 p. 2153 - 2156
反应条件
sodium hydroxide in water
T=0°C; 2 h;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
iodine; N-ethyl-N,N-diisopropylamine; triphenylphosphine in dichloromethane
T=0 - 20°C; 0.5 h;
参考文献
Kumar, Amit; Akula, Hari Kiran; Lakshman, Mahesh K.
European Journal of Organic Chemistry, 2010 , # 14 p. 2709 - 2715
反应条件
1: With gallium; iodobenzene; aluminium
T=120°C; 20 h; Inert atmosphere;
2: (S)-1-phenyl-ethylamine in toluene
T=20°C; 0.166667 h;
3: benzoic acid methyl ester in touene
T=80°C; 3 h;
参考文献
Tang, Xiaoping; Rawson, Daniel; Woodward, Simon
Synlett, 2010 , # 4 art. no. D32709ST, p. 636 - 638
参考文献
Tanaka, Tetsuaki
Journal of the Chinese Chemical Society, 2000 , vol. 47, # 4 B p. 865 - 868
参考文献
Nagao, Yoshimitsu; Yagi, Masahiro; Ikede, Takao; Fujita, Eiichi
Tetrahedron Letters, 1982 , vol. 23, # 2 p. 201 - 204
参考文献
Zhao, Qian-Yi; Yuan, Zhi-Liang; Shia, Min
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 637 - 643
反应条件
disodium hydrogenphosphate; iodine; sodium sulfate
T=65°C; 90 h;
参考文献
Calvet, Sandrine; David, Olivier; Vanucci-Bacque, Corinne; Fargeau-Bellassoued, Marie-Claude; Lhommet, Gerard
Tetrahedron, 2003 , vol. 59, # 33 p. 6333 - 6339
