对硝基苯基-b-D-昆布二糖苷合成路线 （共 11 条）
反应条件
pyranose 2-oxidase; catalase in water T=22°C; 72 h;
参考文献
Freimund, Stefan; Huwig, Alexander; Giffhorn, Friedrich; Koepper, Sabine
Chemistry - A European Journal, 1998 , vol. 4, # 12 p. 2442 - 2455
反应条件
Thermus nonproteolyticus HG102 E338A mutant; glycine; sodium hydroxide in aq. buffer T=45°C; pH=8.8; 48 h; Enzymatic reaction; pH-valueConcentrationTemperature; Overall yield = 96 percent;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
sodium methylate in methanol 7 h; Ambient temperature;
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387
反应条件
E383A mutant β-glucosidase in phosphate buffer T=35°C; pH=7.0; Enzyme kinetics; Further Variations:TemperaturespH-valuesconcentration;
参考文献
Faijes, Magda; Saura-Valls, Marc; Perez, Xavi; Conti, Marta; Planas, Antoni
Carbohydrate Research, 2006 , vol. 341, # 12 p. 2055 - 2065
反应条件
1: methanol; sodium methylate / 20 °C 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
1: pyridine; hydrogen fluoride / -20 - 20 °C 2: methanol; sodium methylate / 20 °C 3: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
1: 45 percent / benzyltriethylammonium chloride, aq. NaOH / CH2Cl2 / 4 h / Heating 2: 62 percent / NaOMe / methanol / 7 h / Ambient temperature View Scheme
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387
反应条件
1: 45 percent / benzyltriethylammonium chloride, aq. NaOH / CH2Cl2 / 4 h / Heating 2: 62 percent / NaOMe / methanol / 7 h / Ambient temperature View Scheme
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387
反应条件
1: 98 percent / HBr / acetic acid / 0.25 h / Ambient temperature 2: 45 percent / benzyltriethylammonium chloride, aq. NaOH / CH2Cl2 / 4 h / Heating 3: 62 percent / NaOMe / methanol / 7 h / Ambient temperature View Scheme
参考文献
Viladot, Josep-Lluis; Moreau, Vincent; Planas, Antoni; Driguez, Hugues
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2383 - 2387
反应条件
Thermus nonproteolyticus HG102 E338A mutant; glycine; sodium hydroxide in water T=45°C; pH=8.8; 24 h; Enzymatic reaction;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
