in ethanol
stoich., to a soln. of metal salt added a soln. of ligand, heated with stirring; ppt. filtered, washed (ice-cold ethanol), dried (silica gel); elem. anal.;
参考文献
Tarafder; Chew, Kar-Beng; Crouse, Karen A.; Ali; Yamin; Fun
Polyhedron, 2002 , vol. 21, # 27-28 p. 2683 - 2690
in ethanol
addn. of Ni(NO3)2 to 2 equiv. of ligand, heating for 10 min; cooling in ice (crystn.), collection, washing (ice-cold alcohol), drying(vac., over silica gel); elem. anal.;
in ethanol
stoich., to a soln. of metal salt added a soln. of ligand, heated with stirring; ppt. filtered, washed (ice-cold ethanol), dried (silica gel); elem. anal.;
参考文献
Tarafder; Chew, Kar-Beng; Crouse, Karen A.; Ali; Yamin; Fun
Polyhedron, 2002 , vol. 21, # 27-28 p. 2683 - 2690
in ethanol
addn. of Cu(NO3)2 to 2 equiv. of ligand, heating for 10 min; cooling in ice (crystn.), collection, washing (ice-cold alcohol), drying(vac., over silica gel); elem. anal.;
in ethanol
stoich., to a soln. of metal salt added a soln. of ligand, heated with stirring; ppt. filtered, washed (ice-cold ethanol), dried (silica gel); elem. anal.;
参考文献
Tarafder; Chew, Kar-Beng; Crouse, Karen A.; Ali; Yamin; Fun
Polyhedron, 2002 , vol. 21, # 27-28 p. 2683 - 2690
in ethanol
addn. of Zn(NO3)2 to 2 equiv. of ligand, heating for 10 min; cooling in ice or refrigerating overnight (crystn.), collection, washing(ice-cold alcohol), drying (vac., over silica gel); elem. anal.;
