1-(4-甲氧基苯基)-1H-苯并咪唑合成路线 (共 15 条)
反应条件
pyridine; water; copper diacetate in N,N-dimethyl-formamide T=30°C; 24 h;
参考文献
Nishiura, Katsutoshi; Urawa, Yoshio; Soda, Shigeru
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1679 - 1684
反应条件
copper(l) iodide; 8-hydroxy-quinoline; bis(tetraethylammonium) carbonate in water; N,N-dimethyl-formamide T=130°C; 16 h;
参考文献
Farahat, Abdelbasset A.; Boykin, David W.
Tetrahedron Letters, 2014 , vol. 55, # 19 p. 3049 - 3051
反应条件
potassium carbonate; bis(μ-iodo)bis[(-)-sparteine]dicopper(I) in dimethyl sulfoxide T=115°C; 7 h;
参考文献
Zhang, Yihua; Yang, Xinye; Xing, Hui; Zhang, Ye; Lai, Yisheng; Jiang, Yongwen; Ma, Dawei
Chinese Journal of Chemistry, 2012 , vol. 30, # 4 p. 875 - 880
反应条件
copper diacetate; tetrabutyl ammonium fluoride; oxygen in N,N-dimethyl-formamide T=20°C; Arylation; 48 h;
参考文献
Lam, Patrick Y. S.; Deudon, Sophie; Averill, Kristin M.; Li, Renhua; He, Ming Y.; DeShong, Philip; Clark, Charles G.
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7600 - 7601
反应条件
hydrogen; pyridinium p-toluenesulfonate; palladium on activated charcoal in ethyl acetate T=20°C; P=2585.74 Torr; 3 h;
参考文献
Hornberger, Keith R.; Adjabeng, George M.; Dickson, Hamilton D.; Davis-Ward, Ronda G.
Tetrahedron Letters, 2006 , vol. 47, # 30 p. 5359 - 5361
反应条件
Cu(II)(MeCOCHCO2Et)2 in water T=40°C; P=760.051 Torr; 96 h;
参考文献
Joubert, Nicolas; Basle, Emmanuel; Vaultier, Michel; Pucheault, Mathieu
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2994 - 2997
反应条件
oxalic acid dihydrazide; phosphoric acid trihydrate; tetrabutylammomium bromide; hexane-2,5-dione; copper(II) oxide in water T=120°C; 48 h;
参考文献
Huang, Manna; Lin, Xiaoqin; Zhu, Xinhai; Peng, Weili; Xie, Jianwei; Wan, Yiqian
European Journal of Organic Chemistry, 2011 , # 24 p. 4523 - 4527
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide T=120°C; 40 h; Schlenk techniqueInert atmosphere;
参考文献
Ke, Chun-Hung; Kuo, Bing-Chiuan; Nandi, Debkumar; Lee, Hon Man
Organometallics, 2013 , vol. 32, # 17 p. 4775 - 4784
反应条件
1: Pd2(dba)3; P(o-tol)3; i-Pr2EtN / dimethylformamide / 20 °C 2: 98 percent / tetrabutylammonium fluoride; Cu(OAc)2; O2 / dimethylformamide / 48 h / 20 °C View Scheme
参考文献
Lam, Patrick Y. S.; Deudon, Sophie; Averill, Kristin M.; Li, Renhua; He, Ming Y.; DeShong, Philip; Clark, Charles G.
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7600 - 7601
反应条件
sodium hydride; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=40°C;
参考文献
Wang, Feng-Yan; Chen, Zhen-Chu; Zheng, Qin-Guo
Journal of Chemical Research, 2004 , # 3 p. 206 - 207