1 -苯基-1H -苯并咪唑合成路线 (共 33 条)
反应条件
iron; ammonium chloride in isopropyl alcohol T=80°C; 2 h;
参考文献
Hanan, Emily J.; Chan, Bryan K.; Estrada, Anthony A.; Shore, Daniel G.; Lyssikatos, Joseph P.
Synlett, 2010 , # 18 p. 2759 - 2764
反应条件
Pt-TiO2 T=32°C; 4 h; UV-irradiationInert atmosphere;
参考文献
Selvam; Swaminathan
Tetrahedron Letters, 2011 , vol. 52, # 26 p. 3386 - 3392
反应条件
caesium carbonate in N,N-dimethyl acetamide T=190°C; 16 h; Microwave irradiation;
参考文献
Diness, Frederik; Fairlie, David P.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 32 p. 8012 - 8016
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide T=120°C; 40 h; Schlenk techniqueInert atmosphere;
参考文献
Ke, Chun-Hung; Kuo, Bing-Chiuan; Nandi, Debkumar; Lee, Hon Man
Organometallics, 2013 , vol. 32, # 17 p. 4775 - 4784
反应条件
1: N-phenyl-para-phenylenediamine With n-butyllithium in diethyl ether T=20°C; 48 h; 2: N,N-dimethyl-formamide in diethyl ether 1 h; Further stages.;
参考文献
Crawford, Lynne A.; McNab, Hamish; Mount, Andrew R.; Wharton, Stuart I.
Journal of Organic Chemistry, 2008 , vol. 73, # 17 p. 6642 - 6646
反应条件
1: Pd2(dba)3; P(o-tol)3; i-Pr2EtN / dimethylformamide / 20 °C 2: 83 percent / tetrabutylammonium fluoride; Cu(OAc)2; O2 / dimethylformamide / 48 h / 20 °C View Scheme
参考文献
Lam, Patrick Y. S.; Deudon, Sophie; Averill, Kristin M.; Li, Renhua; He, Ming Y.; DeShong, Philip; Clark, Charles G.
Journal of the American Chemical Society, 2000 , vol. 122, # 31 p. 7600 - 7601
反应条件
copper diacetate; tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=20°C; 48 h;
参考文献
Lam, Patrick Y.S.; Vincent, Guillaume; Bonne, Damien; Clark, Charles G.
Tetrahedron Letters, 2002 , vol. 43, # 16 p. 3091 - 3094
反应条件
hydrogen; toluene-4-sulfonic acid in toluene T=60°C; P=7757.43 Torr; pH=3; 3 h; Inert atmosphere;
参考文献
Bhor, Malhari D.; Bhanage, Bhalchandra M.
Synthetic Communications, 2010 , vol. 40, # 12 p. 1743 - 1749
反应条件
sodium hydride; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=40°C;
参考文献
Wang, Feng-Yan; Chen, Zhen-Chu; Zheng, Qin-Guo
Journal of Chemical Research, 2004 , # 3 p. 206 - 207
反应条件
[Cu30I16(5-methyl-4-(p-tolyl)pyrimidine-2-thiolato)12(μ10-S4)] in methanol 5 h; Reflux; TemperatureReagent/catalyst;
参考文献
Li, Hong-Xi; Zhao, Wei; Li, Hai-Yan; Xu, Zhong-Lin; Wang, Wen-Xia; Lang, Jian-Ping
Chemical Communications, 2013 , vol. 49, # 39 p. 4259 - 4261