反应条件
in diethyl ether
addn. a suspn. of benzoyl peroxide in ether to a suspn. of Ni(COD)2 and PCy3 (ratio 1:2) in ether at-78°C, stirring for 2 h at 22°C, (Ar); filtn. of ppt. (Ni(OCOPH)2(PCy3)2), washing (ether), drying in vacuum, evapn. of mother soln., treatment of residue with MeOH, filtn. of ppt. (Ni(OCOPh)2, washing (MeOH), drying in vacuo;
参考文献
Isaeva, L. S.; Morozova, L. N.; Kravtsov, D. N.
Inorganica Chimica Acta, 1990 , vol. 171, p. 29 - 34
