in benzene
byproducts: P(O)Ph3, PPh3; excess PCy3 was added under N2 to a slurry of ReOCl3(PPh3)2 in benzene, mixt. was stirred for 1 h; solvent was removed under vac., residue washed several times with Et2O; elem. anal.;
参考文献
Zeiher, E. H. Kelle; DeWit, David G.; Caulton, Kenneth G.
Journal of the American Chemical Society, 1984 , vol. 106, # 23 p. 7006 - 7011