in ethanol byproducts: COD; 1 equiv. of NaBH4, 2 equiv. of phosphine per complex, room temp., few min, gas evolution; evapn., extn. (benzene), recrystn. (benzene/hexane);
in tetrahydrofuran
(argon); NMR tube: addn. of the ligand to the Pt complex in THF at -78°C, slight warming for dissoln., recooling to -80°C; NMR monitoring;
参考文献
Chaloner, Penny A.; Broadwood-Strong, Gillian T. L.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 1039 - 1043
