in chlorobenzene Kinetics; under N2 atm.; fac-(dihapto-(60)fullerene)(dihapto-1,10-phenanthroline)tricarbonyl molybdenum(0) and PPh3 in chlorobenzene at 347.6 K; monitored at 440 nm and by IR spectroscopy;
参考文献
Ocasio-Delgado, Yessenia; De Jesus-Segarra, Jonathan; Cortes-Figueroa, Jose E.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 14 p. 3366 - 3372
in chloroform-d1 byproducts: MeP(O)(PPh)2; under N2; phosphine (5-100 equiv.) added to soln. of Pd complex in CDCl3at 25°C; 24 h; not isolated; monitored by (1)H and (31)P NMR spectra;
参考文献
Stockland Jr., Robert A.; Levine, Adam M.; Giovine, Matthew T.; Guzei, Ilia A.; Cannistra, Joseph C.
Organometallics, 2004 , vol. 23, # 4 p. 647 - 656
in tetrahydrofuran T=40 - 65°C; 1 h; Inert atmosphere; ConcentrationTime;
参考文献
Umicore AG and Co. KG; Doppiu, Angelino; Heil, Beate; Rivas-Nass, Andreas; Woerner, Eileen; Karch, Ralf
Patent: EP2679593 A1, 2014 ;
Location in patent: Paragraph 0070; 0071 ;
→
反应条件
in tetrahydrofuran T=20°C; Equilibrium constant;
参考文献
Abdur-Rashid, Kamaluddin; Fong, Tina P.; Greaves, Bronwyn; Gusev, Dmitry G.; Hinman, Justin G.; Landau, Shaun E.; Lough, Alan J.; Morris, Robert H.
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9155 - 9171
