2-(4-甲氧基苯基)-1H-苯并咪唑合成路线 (共 67 条)
反应条件
iron(III) trichloride on alumina in N,N-dimethyl-formamide
T=38 - 41°C; 2.2 h; Sonication;
参考文献
Chen, Guo-Feng; Dong, Xiao-Yun; Meng, Fan-Zhu; Chen, Bao-Hua; Li, Ji-Tai; Wang, Shu-Xiang; Bai, Guo-Yi
Letters in Organic Chemistry, 2011 , vol. 8, # 7 p. 464 - 469
反应条件
[2,2']bipyridinyl; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper(l) chloride in neat (no solvent)
T=20°C; 13 h; Green chemistry;
参考文献
Yu, Jiatao; Xu, Jian; Lu, Ming
Applied Organometallic Chemistry, 2013 , vol. 27, # 10 p. 606 - 610
反应条件
exo/endo-9-cyclohexyl-9-phospabicyclo[4.2.1]nonane; isobutyldiisopropylamine; [RhCl(cis-cyclooctene)2]2 in tetrahydrofuran; 1,2-dichloro-benzene
T=150°C; 24 h;
参考文献
Lewis, Jared C.; Wu, Jessica Y.; Bergman, Robert G.; Ellman, Jonathan A.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 10 p. 1589 - 1591
反应条件
diisopropylisobutylamine; [RhCl(coe)2]2 in tetrahydrofuran
T=200°C; 2 h; microwave irradiation;
参考文献
Lewis, Jared C.; Berman, Ashley M.; Bergman, Robert G.; Ellman, Jonathan A.
Journal of the American Chemical Society, 2008 , vol. 130, # 8 p. 2493 - 2500
反应条件
copper(ll) bromide in toluene
T=100°C; 24 h;
参考文献
Xiao, Tiebo; Xiong, Shengwei; Xie, Yang; Dong, Xichang; Zhou, Lei
RSC Advances, 2013 , vol. 3, # 36 p. 15592 - 15595
反应条件
2,6-dimethylpyridine; bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl acetamide
T=140°C; P=4912.9 Torr; 24 h;
参考文献
Perry; Wilson
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7016 - 7021
反应条件
2,6-dimethylpyridine; bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl acetamide
T=140°C; P=4912.9 Torr; 24 h;
参考文献
Perry; Wilson
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7016 - 7021
反应条件
silphox [POCl3-n(SiO2)n, silica phosphinoxide] in N,N-dimethyl-formamide
0.133333 h; Microwave irradiation;
参考文献
Hasaninejad, Alireza; Niknam, Khodabakhsh; Zare, Abdolkarim; Farsimadan, Ehsan; Shekouhy, Mohsen
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 1 p. 147 - 155
反应条件
carbon monoxide; 1,10-phenanthroline monohydrate; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=120°C; P=4560.31 Torr; 65.5 h;
参考文献
Hubbard, Jeremiah W.; Piegols, Adam M.; Soederberg, Bjoern C.G.
Tetrahedron, 2007 , vol. 63, # 30 p. 7077 - 7085
反应条件
copper(I) oxide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in N,N-dimethyl-formamide
T=140°C; 16 h; Inert atmosphere;
参考文献
Qu, Yanyang; Pan, Lei; Wu, Zhiqing; Zhou, Xiangge
Tetrahedron, 2013 , vol. 69, # 6 p. 1717 - 1719