hydrogenchloride; hydrogen; palladium 10 on activated carbon in ethanol; water P=760.051 Torr;

1: hydroxylamine hydrochloride; sodium acetate / ethanol / 6 h / 20 °C 2: hydrogenchloride; hydrogen / palladium 10 on activated carbon / ethanol; water / 760.05 Torr View Scheme

in water 1.) 50-60 deg C, 15 min; 2.) 1 h;