1,2-亚甲基双氧-4-硝基苯 合成路线 （共 40 条）
反应条件
nitric acid in acetic acid
参考文献
Hoffmann-La Roche Inc.
反应条件
Bi(NO3)3·5H2O in benzene T=70 - 80°C; 2 h; Inert atmosphere;
参考文献
Yadav, Rammohan R.; Vishwakarma, Ram A.; Bharate, Sandip B.
反应条件
tris-(dibenzylideneacetone)dipalladium(0); t-Bu Brett Phos; TDA; sodium nitrite in tert-butyl alcohol T=130°C; 24 h; regioselective reaction;
参考文献
Fors, Brett P.; Buchwald, Stephen L.
反应条件
nitric acid in water; acetic acid T=3 - 20°C; Nitration; deacetylation; 3.75 h; Title compound not separated from byproducts;
参考文献
McGall, Glenn H.; Barone, Anthony D.; Diggelmann, Martin; Fodor, Stephen P. A.; Gentalen, Erik; Ngo, Nam
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; zirconium tetra-t-butoxide in dichloromethane 4 h; Ambient temperature;
参考文献
Krohn, Karsten; Kuepke, Jochen; Rieger, Hagen
反应条件
potassium carbonate in dimethyl sulfoxide T=55°C; 6 h;
参考文献
Ikeya, Yukinobu; Taguchi, Heihachiro; Yoshioka, Itiro
参考文献
Mameli
反应条件
nitric acid T=25°C; 1 h;
参考文献
Takakis, Ioannis M.; Hadjimihalakis, Phaedon M.
133-03-9 5-[(1R,3aR,4S,6aR)-4-(1,3-苯并二氧戊环-5-基)-1,3,3a,4,6,6a-六氢呋喃并[4,3-c]呋喃-1-基]-1,3-苯并二氧戊环
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反应条件
反应条件
nitric acid; acetic acid T=20 - 40°C;
参考文献
Boeeseken; Cohen
参考文献
Ekeley; Klemme
