1-氯-N,N,2-三甲基丙烯胺合成路线 (共 13 条)
反应条件
(i) HCl, COCl2, CHCl3, (ii) Et3N; Multistep reaction;
参考文献
Bendall, Justin G.; Payne, Andrew N.; Screen, Thomas E. O.; Holmes, Andrew B.
Chemical Communications, 1997 , # 11 p. 1067 - 1068
反应条件
trimethylamine in pentane T=-78 - 4°C;
参考文献
O'Brien, Jeannette M.; Kingsbury, Jason S.
Journal of Organic Chemistry, 2011 , vol. 76, # 6 p. 1662 - 1672
反应条件
phenylphosphonous dichloride in chloroform
参考文献
Weingarten,H.
Journal of Organic Chemistry, 1970 , vol. 35, p. 3970 - 3971
反应条件
in chloroform 6 h; Ambient temperature; Product distribution;
参考文献
Ernst, Beat.; Winkler, Tammo.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3081 - 3084
反应条件
in chloroform; ethyl acetate; Petroleum ether
参考文献
Ciba-Geigy Corporation
Patent: US5218097 A1, 1993 ;
反应条件
in chloroform; ethyl acetate; Petroleum ether
参考文献
Ciba-Geigy Corporation
Patent: US5218097 A1, 1993 ;
参考文献
Ciba-Geigy Corporation
Patent: US5218097 A1, 1993 ;
反应条件
pyridine in tetrahydrofuran; methanol; water
参考文献
Ciba-Geigy Corporation
Patent: US4931581 A1, 1990 ;
参考文献
Devos,A. et al.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 1180 - 1181
参考文献
Devos,A. et al.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 1180 - 1181