N-(4-溴苯基)甲酰胺合成路线 (共 37 条)
反应条件
sodium formate T=20°C; 2.75 h; Neat (no solvent);
参考文献
Brahmachari, Goutam; Laskar, Sujay
Tetrahedron Letters, 2010 , vol. 51, # 17 p. 2319 - 2322
反应条件
choline chloride*2SnCl2 in water T=70°C;
参考文献
Azizi, Najmadin; Gholibeglo, Elham; Babapour, Mahbobe; Ghafuri, Hossein; Bolourtchian, Seyed Mohammad
Comptes Rendus Chimie, 2012 , vol. 15, # 9 p. 768 - 773
反应条件
caesium carbonate T=70°C; 14 h;
参考文献
Fakhri, Parisa; Jaleh, Babak; Nasrollahzadeh, Mahmoud
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 383-384, p. 17 - 22
反应条件
formic acid; acetic anhydride in tetrahydrofuran
参考文献
Bunker, Amy Mae; Harter, William Glen; Hicks, James Lester; O'Brien, Patrick Michael; Pham, Ly; Picard, Joseph Armand; Roark, William Howard
Patent: US2003/144274 A1, 2003 ;
US 20030144274 A1
反应条件
oxygen; Mn(OAc)3•2H2O in toluene T=90°C; P=760.051 Torr; 12 h;
参考文献
Zhang, Chun; Xu, Zejun; Shen, Tao; Wu, Guolin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2012 , vol. 14, # 9 p. 2362 - 2365
反应条件
supported 2-(sulfooxy)propane-1,2,3-tricarboxylic acid on silica gel T=20°C; 13 h; Neat (no solvent);
参考文献
Ghorbani-Choghamarani, Arash; Akbaripanah, Ziba
Chinese Chemical Letters, 2012 , vol. 23, # 4 p. 450 - 453
反应条件
in tetrahydrofuran T=-20°C; 0.25 h;
参考文献
Krishnamurthy, S.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3315 - 3318
反应条件
1: formic acid; acetic anhydride T=55°C; 2 h; 2: 4-bromo-aniline in tetrahydrofuran T=20°C; 3 h;
参考文献
GLAXO GROUP LIMITED
Patent: WO2003/99786 A2, 2003 ;
Location in patent: Page 44-45 ;
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide; bis(benzonitrile)palladium(II) dichloride; triphenylphosphine in xylene T=90°C; Formylation; 4 h;
参考文献
Lapidus; Petrovskii; Bruk; Beletskaya
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 11 p. 1636 - 1639
反应条件
palladium on activated charcoal in acetonitrile 12 h; Heating;
参考文献
Reddy, P.Ganapati; Baskaran
Tetrahedron Letters, 2002 , vol. 43, # 10 p. 1919 - 1922