Jone's reagent in acetone T=0°C; 8 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Nandanan; Jayachandran; Phukan, Prodeep; Pais, Godwin C. G.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 12 p. 1221 - 1227
1: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
T=20°C; 0.5 h;
2: With sodium tetrahydroborate; water in tetrahydrofuran
T=0°C; 0.5 h;
Sulfolobus solfataricus alcohol dehydrogenase-10; nicotinamide adenine dinucleotide in ethanol
T=80°C; pH=9; 18 h; Inert atmosphereaq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Friest, Jacob A.; Maezato, Yukari; Broussy, Sylvain; Blum, Paul; Berkowitz, David B.
Journal of the American Chemical Society, 2010 , vol. 132, # 17 p. 5930 - 5931
